Technology Process of C33H50O5Si
There total 3 articles about C33H50O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ruthenium trichloride; sodium periodate;
In
dichloromethane; acetonitrile;
at 5 - 20 ℃;
for 3.5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / diethyl ether / 35 °C / Inert atmosphere; Reflux
1.2: 1 h / 20 °C
1.3: Cooling with ice
2.1: triethylamine; dmap / 14 h / 20 °C
2.2: 14 h / 20 °C
3.1: sodium periodate; ruthenium trichloride / dichloromethane; acetonitrile / 3.5 h / 5 - 20 °C
With
dmap; ruthenium trichloride; sodium periodate; magnesium; triethylamine;
In
diethyl ether; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; dmap / 14 h / 20 °C
1.2: 14 h / 20 °C
2.1: sodium periodate; ruthenium trichloride / dichloromethane; acetonitrile / 3.5 h / 5 - 20 °C
With
dmap; ruthenium trichloride; sodium periodate; triethylamine;
In
dichloromethane; acetonitrile;