2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

Base Information

Chemical Name:2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide
CAS No.:202867-18-3
Molecular Formula:C₁₄H₁₂BrN₅O₂S
Molecular Weight:394.252
Hs Code.:

Synonyms:2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

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Chemical Property of 2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

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Technology Process of 2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

There total 3 articles about 2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 202867-16-1
ethyl 2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)acetate

: 202867-18-3
2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;

Reference yield:

: 60870-40-8
4-(4-Bromo-phenyl)-5-furan-2-yl-4H-[1,2,4]triazole-3-thiol

: 202867-18-3
2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / KOH / ethanol / 2 h / Heating

2: 83 percent / hydrazine hydrate / ethanol / 3 h / Heating

With potassium hydroxide; hydrazine hydrate; In ethanol;

Reference yield:

: 3326-71-4
2-furoic acid hydrazide

: 202867-18-3
2-((4-(4-bromophenyl)-5-(furan-2-yl)-4H-1,2,4-triazol-3-yl)thio)aceto hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 2 h / Reflux

2: sodium hydroxide / water / 2 h / Reflux

3: potassium hydroxide / ethanol / 2 h / Reflux

4: hydrazine hydrate / ethanol / 3 h / Reflux

With hydrazine hydrate; potassium hydroxide; sodium hydroxide; In ethanol; water;
DOI:10.1002/jhet.4159