C₂₂H₂₇NO₂

Base Information

Chemical Name:C₂₂H₂₇NO₂
CAS No.:1266568-69-7
Molecular Formula:C₂₂H₂₇NO₂
Molecular Weight:337.462
Hs Code.:

C<sub>22</sub>H<sub>27</sub>NO<sub>2</sub>

Synonyms:C₂₂H₂₇NO₂

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Chemical Property of C₂₂H₂₇NO₂

Chemical Property:

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Technology Process of C₂₂H₂₇NO₂

There total 7 articles about C₂₂H₂₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: C₁₉H₂₁NO₃

: 24470-78-8
isopropyltriphenylphosphonium iodide

: 1266568-69-7
C₂₂H₂₇NO₂

Guidance literature:: isopropyltriphenylphosphonium iodide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.5h; Inert atmosphere;

C₁₉H₂₁NO₃; In tetrahydrofuran; hexane; at -40 - 0 ℃; Inert atmosphere;
DOI:10.1002/chem.201002287

Reference yield:

: 1038778-89-0
(2-iodo-5-methoxyphenyl)carbamic acid 1,1-dimethylethyl ester

: 1266568-69-7
C₂₂H₂₇NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tetrabutylammomium bromide; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 20 - 100 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.67 h / -78 °C / Inert atmosphere

5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

5.2: -40 - 0 °C / Inert atmosphere

With tetrabutylammomium bromide; palladium diacetate; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 2.1: Heck reaction / 5.2: Wittig reaction;
DOI:10.1002/chem.201002287

Reference yield:

: C₂₄H₂₇NO₅

: 1266568-69-7
C₂₂H₂₇NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.67 h / -78 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

3.2: -40 - 0 °C / Inert atmosphere

With potassium hexamethylsilazane; diisobutylaluminium hydride; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; toluene; 3.2: Wittig reaction;
DOI:10.1002/chem.201002287