S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

Base Information

Chemical Name:S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate
CAS No.:1085994-46-2
Molecular Formula:C₁₈H₂₀INOS
Molecular Weight:425.333
Hs Code.:

Synonyms:S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

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Chemical Property of S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

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Technology Process of S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

There total 7 articles about S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1085994-41-7
(R)-S-ethyl-3-benzyl-4-phenyloxazolidin-2-thionium triflate

: 1085994-46-2
S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

Guidance literature:: (R)-S-ethyl-3-benzyl-4-phenyloxazolidin-2-thionium triflate; With lithium trifluoromethanesulfonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With rubidium iodide; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.3987/COM-08-11410

Reference yield:

: 1085994-41-7
(R)-S-ethyl-3-benzyl-4-phenyloxazolidin-2-thionium triflate

: 1085994-55-3
(R)-3-benzyl-4-phenylthiazolidin-2-one

: 1085994-46-2
S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

: (R)-(-)-N-benzyl-4-phenyloxazolidin-2-one

Guidance literature:: With lithium iodide; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.3987/COM-08-11410

Reference yield:

: 56613-80-0
D-2-phenylglycinol

: 1085994-46-2
S-ethyl N-benzyl-N-(R)-2-iodo-1-phenylethylcarbamathioate

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / 5 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 0.67 h / 20 °C

3.1: dichloromethane / 5 h / 20 °C

4.1: acetonitrile / 0.5 h / 20 °C

5.1: lithium trifluoromethanesulfonate / N,N-dimethyl-formamide / 0.5 h / 0 °C / Molecular sieve; Inert atmosphere

5.2: Inert atmosphere

With sodium tetrahydroborate; lithium trifluoromethanesulfonate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-08-11410