1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

Base Information

Chemical Name:1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide
CAS No.:494771-03-8
Molecular Formula:C₄₅H₆₈N₁₂O₁₂
Molecular Weight:969.108
Hs Code.:

1-[19-amino-5-<i>sec</i>-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

Synonyms:1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

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Chemical Property of 1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

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Technology Process of 1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

There total 2 articles about 1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.4%

: C₆₂H₈₁N₁₂O₁₄Pol

: 494771-03-8
1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

: 1-[19-amino-5-sec-butyl-8-(2-carbamoyl-ethyl)-11-carbamoylmethyl-2-(4-hydroxy-benzyl)-3,6,9,12,20-pentaoxo-1,4,7,10,13pentaaza-cycloeicos-16-ene-14-carbonyl]-pyrrolidine-2-carboxylic acid [1-(carbamoylmethyl-carbamoyl)-3-methyl-butyl]-amide

Guidance literature:: C₆₂H₈₁N₁₂O₁₄Pol; With Hoveyda-Grubbs catalyst second generation; In dichloromethane; for 24h; rink amide resin Inert atmosphere; Reflux;

With dimethyl sulfoxide; In dichloromethane; for 12h; rink amide resin Reagent/catalyst; Solvent; Further stages; Inert atmosphere; Reflux;
DOI:10.1039/c2ob26938d