4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

Base Information

Chemical Name:4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide
CAS No.:94418-20-9
Molecular Formula:C₂₉H₂₄ClN₃O₆S
Molecular Weight:578.045
Hs Code.:

Synonyms:4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

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Chemical Property of 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

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Technology Process of 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

There total 6 articles about 4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 94418-11-8
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole

: 94418-20-9
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

Guidance literature:: With monopermaleic acid; In chloroform; for 18h; Ambient temperature;
DOI:10.1002/jhet.5570210435

Reference yield:

: 76-83-5
trityl chloride

: 94418-20-9
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / Triethylamine / dimethylformamide / 24 h

2: 94 percent / 35percent aq. NaOH / ethanol / 3 h / 25 °C

3: 82 percent / Triethylamine / dimethylformamide / overnight

4: 83 percent / Permaleic Acid / CHCl₃ / 18 h / Ambient temperature

With sodium hydroxide; monopermaleic acid; triethylamine; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210435

Reference yield:

: 94418-08-3
4-<(Z)-1-Carbethoxy-1-hydroxyimino>methyl-2-chloroacetamidothiazole

: 94418-20-9
4-<(Z)-1-Acetonyloxycarbonyl-1-trityloxyimino>methyl-2-chloroacetamidothiazole N-Oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / Triethylamine / dimethylformamide / 24 h

2: 94 percent / 35percent aq. NaOH / ethanol / 3 h / 25 °C

3: 82 percent / Triethylamine / dimethylformamide / overnight

4: 83 percent / Permaleic Acid / CHCl₃ / 18 h / Ambient temperature

With sodium hydroxide; monopermaleic acid; triethylamine; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570210435