2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

Base Information

Chemical Name:2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol
CAS No.:1463523-04-7
Molecular Formula:C₂₇H₂₇NO₃
Molecular Weight:413.516
Hs Code.:

Synonyms:2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

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Chemical Property of 2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

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Technology Process of 2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

There total 5 articles about 2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: C₂₄H₂₅NO₃

: 106-96-7
propargyl bromide

: 1463523-04-7
2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium carbonate; In acetone; toluene; for 2.5h; Reflux;
DOI:10.1039/c3cc44799e

Reference yield:

: 89-57-6
5-Aminosalicylic Acid

: 1463523-04-7
2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: Acidic conditions

2: triethylamine

3: Neutral conditions

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

5: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

With lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; triethylamine; In tetrahydrofuran; acetone; toluene; 2: |Grignard Reaction;
DOI:10.1039/c3cc44799e

Reference yield:

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 1463523-04-7
2-(6-(ethyl(prop-2-yn-1-yl)amino)-4,4-diphenyl-4H-benzo[d][1,3]dioxin-2-yl)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine

2: Neutral conditions

3: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

4: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

With lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; triethylamine; In tetrahydrofuran; acetone; toluene; 1: |Grignard Reaction;
DOI:10.1039/c3cc44799e