Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

Base Information

Chemical Name:Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside
CAS No.:90132-67-5
Molecular Formula:C₁₉H₂₇BrO₇
Molecular Weight:447.323
Hs Code.:

Synonyms:Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

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Chemical Property of Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

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Technology Process of Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

There total 2 articles about Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 90132-66-4
Methyl 4,6-O-Benzylidene-2-deoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

: 90132-67-5
Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 0.666667h; Heating;
DOI:10.1021/jo00187a008

Reference yield:

: 75879-81-1
Methyl 4,6-O-Benzylidene-2-deoxy-2-C-methyl-α-D-allopyranoside

: 90132-67-5
Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Sodium hydride / diethyl ether / 3 h / Heating

2: 94 percent / N-Bromosuccinimide, Barium carbonate / CCl₄ / 0.67 h / Heating

With N-Bromosuccinimide; sodium hydride; barium carbonate; In tetrachloromethane; diethyl ether;
DOI:10.1021/jo00187a008

Reference yield: 73.0%

: 90132-67-5
Methyl 4-O-Benzoyl-6-bromo-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

: 90132-68-6
Methyl 4-O-Benzoyl-2,6-dideoxy-2-C-methyl-3-O-((2-methoxyethoxy)methyl)-α-D-allopyranoside

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In methanol; for 23h; under 760 Torr;
DOI:10.1021/jo00187a008