2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

Base Information

Chemical Name:2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine
CAS No.:1289560-55-9
Molecular Formula:C₂₇H₂₁NO₃S₂
Molecular Weight:471.601
Hs Code.:

Synonyms:2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

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Chemical Property of 2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

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Technology Process of 2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

There total 5 articles about 2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1289560-23-1
2-{2-[(E)-2-(phenylsulfinyl)vinyl]phenylsulfinyl}pyridine

: 1289560-55-9
2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; In 1,2-dichloro-ethane; at 110 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201003633

Reference yield:

: 109-04-6
2-bromo-pyridine

: 1289560-55-9
2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 18 h / 110 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

3: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere

4: [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere

With dipotassium peroxodisulfate; [bis(acetoxy)iodo]benzene; palladium diacetate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633

Reference yield:

: 3111-54-4
2-phenylsulfanylpyridine

: 1289560-55-9
2-{2-[(E)-2-(phenylsulfinyl)vinyl]-6-[(E)-styryl]phenylsulfinyl}pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

2: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere

3: [bis(acetoxy)iodo]benzene; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere

With dipotassium peroxodisulfate; [bis(acetoxy)iodo]benzene; palladium diacetate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633