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Technology Process of {PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

Base Information
  • Chemical Name:{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}
  • CAS No.:143021-68-5
  • Molecular Formula:C28H26Cl2P2Pt
  • Molecular Weight:690.448
  • Hs Code.:
{PtCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}

Synonyms:{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

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Chemical Property of {PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}
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Technology Process of {PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

There total 2 articles about {PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

{PtCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2CCH<sub>2</sub>}
143021-64-1

{PtCl2((C6H5)2PCH2)2CCH2}

{PtCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}
143021-68-5

{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

Guidance literature:
With hydrogenchloride; sodium ethanolate; In ethanol; refluxing the Pt complex in EtOH with a NaOEt satd. soln. in EtOH (15 min), colour change to very dark red, dropwise addn. of a concd. HCl soln., discharge of most of the colour; removing solvent (vac.), extg. (CH2Cl2), passing through a Florisil column, evapg. solvent, crystn., recrystn. (EtOH); elem. anal.;
DOI:10.1039/DT9920001929

Reference yield:

{PtCl<sub>4</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}*0.25CH<sub>2</sub>Cl<sub>2</sub>

{PtCl4((C6H5)2PCH2C(CH3)CHP(C6H5)2)}*0.25CH2Cl2

{PtCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}
143021-68-5

{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

Guidance literature:
In dimethyl sulfoxide; decompn. in DMSO soln. to the Pt(II) complex over several d; not isolated; detn. by NMR;
DOI:10.1039/DT9920001929

Reference yield: 87.0%

{PtCl<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}
143021-68-5

{PtCl2((C6H5)2PCH2C(CH3)CHP(C6H5)2)}

{PtCl<sub>4</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>C(CH<sub>3</sub>)CHP(C<sub>6</sub>H<sub>5</sub>)2)}*0.25CH<sub>2</sub>Cl<sub>2</sub>

{PtCl4((C6H5)2PCH2C(CH3)CHP(C6H5)2)}*0.25CH2Cl2

Guidance literature:
With dichloromethane; chlorine; In dichloromethane; addn. of Cl2 in CCl4 to a stirred soln. of the dichloride in CH2Cl2, immediate colour change to yellow, stirring (20 min), crystn.; filtration, washing (CCl4), drying; elem. anal.;
DOI:10.1039/DT9920001929
upstream raw materials:

{PtCl2((C6H5)2PCH2)2CCH2}

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