trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

Base Information

Chemical Name:trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside
CAS No.:100638-55-9
Molecular Formula:C₅₂H₅₈O₁₃
Molecular Weight:894.001
Hs Code.:

Synonyms:trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

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Technology Process of trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

There total 12 articles about trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 100638-54-8
trideuteriomethyl 2,3,4-tri-O-benzyl-β-D-mannopyranoside

: 100759-62-4
2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl bromide

: 100638-55-9
trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-bemzyl-β-D-mannopyranosyl)-β-D-mannopyranoside

Guidance literature:: With Tl-zeolite 3A; In dichloromethane; for 40h; Ambient temperature; further reagent Ag-zeolite 3A, Ag triflate, HgBr₂/Hg(CN)2;

Reference yield:

: 65827-57-8
1,2,6-tri-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranose

: 100638-55-9
trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: HBr / CH₂Cl₂ / 3 h / 0 °C

2: thallium zeolite / CH₂Cl₂ / 92 h / Ambient temperature; comparison of various promoters on anomer rates

With thallium zeolite; hydrogen bromide; In dichloromethane;
DOI:10.1016/S0008-6215(00)90207-6

Reference yield:

: 65556-30-1
1,6-di-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 100638-55-9
trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: HBr / CH₂Cl₂ / 2 h / 0 °C

2: Ag zeolite / CH₂Cl₂ / 2 h

3: 75 percent / sodium methoxide / methanol / 2 h / Ambient temperature

4: thallium zeolite / CH₂Cl₂ / 92 h / Ambient temperature; comparison of various promoters on anomer rates

With Ag Zeolite; thallium zeolite; hydrogen bromide; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90207-6