2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene

Base Information

• Chemical Name: 2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene
• CAS No.: 1015072-92-0
• Molecular Formula: C₃₅H₃₀O₂
• Molecular Weight: 482.622

Synonyms:2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene

Chemical Property of 2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene

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Technology Process of 2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene

There total 1 articles about 2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

[4-(1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalen-2-yl)but-1-yl-1-yl][tris(1-methylethyl)]silane (1015072-90-8) → 2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene (1015072-92-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/jo701997p

Reference yield: 63.0%

2-but-3-yn-1-yl-1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalene (1015072-92-0) → (P,3S)-14-methoxy-3-methyl-4-(4-methylphenyl)-1,3,6,7-tetrahydrobenzo[c]benzo[5,6]phenanthro[4,3-e]oxepine + (M,3S)-14-methoxy-3-methyl-4-(4-methylphenyl)-1,3,6,7-tetrahydrobenzo[c]benzo[5,6]phenanthro[4,3-e]oxepine

Guidance literature:

With triphenylphosphine; dicarbonylcyclopentadienylcobalt; In decane; at 140 ℃;

DOI:10.1021/jo701997p

upstream raw materials:

[4-(1-{[2-methoxy-6-({[(1S)-1-methyl-3-(4-methylphenyl)prop-2-yl-1-yl]oxy}methyl)phenyl]ethynyl}naphthalen-2-yl)but-1-yl-1-yl][tris(1-methylethyl)]silane

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