C₅₁H₆₂O₁₅SSi

Base Information

Chemical Name:C₅₁H₆₂O₁₅SSi
CAS No.:1286209-84-4
Molecular Formula:C₅₁H₆₂O₁₅SSi
Molecular Weight:975.196
Hs Code.:

C<sub>51</sub>H<sub>62</sub>O<sub>15</sub>SSi

Synonyms:C₅₁H₆₂O₁₅SSi

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Chemical Property of C₅₁H₆₂O₁₅SSi

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Technology Process of C₅₁H₆₂O₁₅SSi

There total 5 articles about C₅₁H₆₂O₁₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286209-83-3
C₄₄H₅₈O₁₄Si

: 1005-56-7
phenylcarbonochloridothioate

: 1286209-84-4
C₅₁H₆₂O₁₅SSi

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 16.5h;
DOI:10.1002/chem.201003399

Reference yield:

: 1204206-79-0
C₄₃H₅₀O₁₄

: 1286209-84-4
C₅₁H₆₂O₁₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethyl acetate / 24 h / 20 °C / 750.08 Torr

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1.5 h / -78 - -10 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -13 - 0 °C

3.2: -78 °C

3.3: -78 - -10 °C

4.1: dmap / dichloromethane / 16.5 h / 0 - 20 °C

With dmap; n-butyllithium; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; 2.1: Swern oxidation;
DOI:10.1002/chem.201003399

Reference yield:

: C₃₆H₄₂O₁₄

: 1286209-84-4
C₅₁H₆₂O₁₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -13 - 0 °C

1.2: -78 °C

1.3: -78 - -10 °C

2.1: dmap / dichloromethane / 16.5 h / 0 - 20 °C

With dmap; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/chem.201003399