1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane

Base Information

Chemical Name:1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane
CAS No.:72008-25-4
Molecular Formula:C₁₀H₁₆O₂
Molecular Weight:168.236
Hs Code.:
European Community (EC) Number:615-703-3
DSSTox Substance ID:DTXSID501267933

Synonyms:72008-25-4;3-(1-ethoxyethoxy)-3-methylpent-1-en-4-yne;3-(1-Ethoxyethoxy)-3-methyl-1-penten-4-yne;1-ETHOXY-1-[(3-METHYLPENT-1-EN-4-YN-3-YL)OXY]ETHANE;SCHEMBL8831478;NSVFPEGYFRAXRT-UHFFFAOYSA-N;DTXSID501267933;MFCD31665300;EN300-1720116;1-ethoxy-1-[3-methyl-4-penten-1-yn-3-oxy]ethane

Suppliers and Price of 1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane

Chemical Property:

Vapor Pressure:0.422mmHg at 25°C
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:168.115029749
Heavy Atom Count:12
Complexity:189

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(C)OC(C)(C=C)C#C

Technology Process of 1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane

There total 1 articles about 1-Ethoxy-1-[(3-methylpent-1-EN-4-YN-3-YL)oxy]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.8%

: 3230-69-1
3-methyl-1-penten-4-yn-3-ol

: 109-92-2,25104-37-4
ethyl vinyl ether

: 72008-25-4
3-(1-ethoxyethoxy)-3-methyl-1-penten-4-yne

Guidance literature:: 3-methyl-1-penten-4-yn-3-ol; ethyl vinyl ether; With toluene-4-sulfonic acid; at 5 - 20 ℃; for 3h;

With triethylamine;

Reference yield:

: 72008-25-4
3-(1-ethoxyethoxy)-3-methyl-1-penten-4-yne

: 169124-54-3
(S)-4-tert-butyldimethylsilyloxy-2,6,6-trimethyl-2-cyclohexenone

: C₂₅H₄₄O₄Si

Guidance literature:: 3-(1-ethoxyethoxy)-3-methyl-1-penten-4-yne; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 2h;

(S)-4-tert-butyldimethylsilyloxy-2,6,6-trimethyl-2-cyclohexenone; In tetrahydrofuran; at -78 - -25 ℃; for 4h;

Reference yield:

: 20013-73-4
2,6,6-trimethylcyclohex-2-en-1-one

: 72008-25-4
3-(1-ethoxyethoxy)-3-methyl-1-penten-4-yne

: 63184-57-6
1-ethoxy-[1-(2,6,6-trimethyl-1-hydroxy-2-cyclohexen-1-yl)-3-methyl-4-penten-1-yn-3-oxy]ethane

Guidance literature:: With n-butyllithium; Multistep reaction; 1.) a) hexane, ether, -60 deg C, b) 0 deg C, 5 min, 2.) a) 20 deg C, b) RT, 1 h;
DOI:10.1021/jo00132a028