Technology Process of (E)-methyl 1-(naphthalen-2-yl)-2-styrylcyclopropanecarboxylate
There total 4 articles about (E)-methyl 1-(naphthalen-2-yl)-2-styrylcyclopropanecarboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
dirhodium tetraacetate;
In
toluene;
at 20 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 5 h / 0 °C
1.2: 17 h / 0 °C / Inert atmosphere
2.1: dirhodium tetraacetate / toluene / 3 h / 20 °C / Inert atmosphere
With
potassium tert-butylate;
dirhodium tetraacetate;
In
tetrahydrofuran; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetyl chloride / 0 - 20 °C / Inert atmosphere
2: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0 - 20 °C / Inert atmosphere
3: dirhodium tetraacetate / toluene / 3 h / 20 °C / Inert atmosphere
With
4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride;
dirhodium tetraacetate;
In
toluene; acetonitrile;
