Technology Process of C44H65NO12
There total 7 articles about C44H65NO12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
DOI:10.1021/jal086112
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 4.5 h / 20 °C
2: (benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
With
(benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/jal086112
- Guidance literature:
-
Multi-step reaction with 4 steps
1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 32 h / 40 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 4.5 h / 20 °C
4: (benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C
With
(benzotriazole-1-yloxy)tris(pyrrolidino)phosphonium hexafluorophosphate; carbon tetrabromide; palladium 10% on activated carbon; hydrogen; potassium carbonate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jal086112
