1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

Base Information

Chemical Name:1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone
CAS No.:80426-73-9
Molecular Formula:C₁₉H₂₉NO₃
Molecular Weight:319.444
Hs Code.:

Synonyms:1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

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Chemical Property of 1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

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Technology Process of 1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

There total 6 articles about 1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 345300-15-4
1-<2-(3,4-dimethoxyphenyl)-2-hydroxyethyl>-5-(1,1-dimethylethyl)-2-piperidone

: 80426-73-9
1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: With perchloric acid; hydrogen; palladium on activated charcoal; In ethanol; at 29 - 30 ℃; for 10h; under 2508 - 2584 Torr;
DOI:10.1248/cpb.29.2691

Reference yield: 89.0%

: 70451-67-1
1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2(1H)-pyridone

: 80426-73-9
1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: With hydrogen; Raney Ni W-2; In ethanol; at 21 ℃; for 9h;
DOI:10.1248/cpb.29.2691

Reference yield:

: 38031-78-6
3-tert-butylpyridine

: 80426-73-9
1-(3,4-dimethoxyphenethyl)-5-(1,1-dimethylethyl)-2-piperidone

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / benzene / 48 h / Ambient temperature

2: 1.) hydrogen, 2.) NaBH₄, 2 N aq. NaOH / 1.) Pt / 1.) ethanol, 25 deg C, 15 h, 2.) ethanol, rt

3: mercuric acetate-ethylenediaminetetraacetic acid / aq. acetic acid / 1.5 h / Heating

4: 100 percent / hydrogen, 70 percent aq. HClO₄ / 10 percent Pd-C / ethanol / 10 h / 29 - 30 °C / 2508 - 2584 Torr

With sodium hydroxide; sodium tetrahydroborate; perchloric acid; ethylenediaminetetraacetic acid; mercury(II) diacetate; hydrogen; palladium on activated charcoal; platinum; In ethanol; acetic acid; benzene;
DOI:10.1248/cpb.29.2691