(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Base Information

Chemical Name:(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid
CAS No.:1383927-17-0
Molecular Formula:C₁₁H₉ClN₄O₄S
Molecular Weight:328.736
Hs Code.:

Synonyms:(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Suppliers and Price of (E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

There total 3 articles about (E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 14160-96-4
4-chloro-6-(phenylamino)pyrimidine-5-carbaldehyde

: 1383927-17-0
(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Guidance literature:: With hydroxylamine-O-sulfonic acid; In acetonitrile; at 20 ℃; for 16h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol301561a

Reference yield:

: 62-53-3
aniline

: 1383927-17-0
(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / chloroform / 1 h / 0 °C / Inert atmosphere

2: hydroxylamine-O-sulfonic acid / acetonitrile / 16 h / 20 °C / Inert atmosphere; Molecular sieve

With triethylamine; hydroxylamine-O-sulfonic acid; In chloroform; acetonitrile;
DOI:10.1021/ol301561a

Reference yield:

: 5305-40-8
2,6-dichloro-pyrimidine carbaldehyde

: 1383927-17-0
(E)-(4-chloro-6-(phenylamino)pyrimidin-5-yl)methyleneaminooxysulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / chloroform / 1 h / 0 °C / Inert atmosphere

2: hydroxylamine-O-sulfonic acid / acetonitrile / 16 h / 20 °C / Inert atmosphere; Molecular sieve

With triethylamine; hydroxylamine-O-sulfonic acid; In chloroform; acetonitrile;
DOI:10.1021/ol301561a