(2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

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Chemical Name:(2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid
CAS No.:1373416-88-6
Molecular Formula:C₅₃H₅₆O₉
Molecular Weight:837.022
Hs Code.:

Synonyms:(2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

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Chemical Property of (2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

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Technology Process of (2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

There total 1 articles about (2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373416-73-9
(S)-3-cyclohexyl-2-(7-hydroxynaphthalen-2-yloxy)propionic acid methyl ester

: 74808-09-6,90357-89-4,90358-01-3,103368-01-0,103368-04-3,103368-06-5,104048-30-8,104048-33-1,114743-70-3,132201-75-3,132748-02-8,83441-60-5
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate

: 1373416-90-0
(2S)-3-cyclohexyl-2-[2-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)naphthalen-7-yloxy]propionic acid

: 1373416-88-6
(2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

Guidance literature:: (S)-3-cyclohexyl-2-(7-hydroxynaphthalen-2-yloxy)propionic acid methyl ester; 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With zinc(II) chloride; In dichloromethane; at 20 ℃; for 2h; Molecular sieve; Inert atmosphere;

With sodium hydroxide; In 1,4-dioxane; methanol; at 20 ℃; for 3h; Overall yield = 19 %; Overall yield = 29 mg;
DOI:10.3998/ark.5550190.0013.311

Reference yield: 61.0%

: 1373416-88-6
(2S)-3-cyclohexyl-2-[2-hydroxy-1-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

: 1373416-92-2
(2S)-3-cyclohexyl-2-[2-hydroxy-1-(α-D-mannopyranosyl)naphthalen-7-yloxy]propionic acid

Guidance literature:: With 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; at 20 ℃; under 7500.75 Torr; Autoclave;
DOI:10.3998/ark.5550190.0013.311