5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

Base Information

Chemical Name:5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole
CAS No.:1595276-32-6
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

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Chemical Property of 5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

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Technology Process of 5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

There total 1 articles about 5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75-11-6
diiodomethane

: 5-((1R,2S)-1-(3,4-dimethoxyphenyl)-4-methoxy-2-methylbut-3-en-1-yl)benzo[d][1,3]dioxole

: 1595276-32-6
5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

Guidance literature:: diiodomethane; With diethylzinc; trifluoroacetic acid; In hexane; dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

5-((1R,2S)-1-(3,4-dimethoxyphenyl)-4-methoxy-2-methylbut-3-en-1-yl)benzo[d][1,3]dioxole; In hexane; dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201307659

Reference yield: 97.0%

: 1595276-32-6
5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

: 78869-00-8
(7'R,8'S)-7'-(3',4'-dimethoxyphenyl)-8,8'-dimethyl-7',8'-dihydronaphtho[4,5-d][1,3]dioxole

Guidance literature:: With hydrogenchloride; In methanol; water; for 1h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201307659

Reference yield:

: 1595276-32-6
5-((1R,2S)-1-(3,4-dimethoxyphenyl)-2-(2-methoxycyclopropyl)propyl)benzo[d][1,3]dioxole

: C₂₁H₂₄O₄

: 3738-02-1,4892-34-6,80483-37-0,102849-09-2
(+) galcatin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol; water / 1 h / Inert atmosphere; Reflux

2: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; ethanol; water;
DOI:10.1002/anie.201307659