phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

Base Information

Chemical Name:phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester
CAS No.:913620-75-4
Molecular Formula:C₂₆H₃₃O₈P
Molecular Weight:504.517
Hs Code.:

phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-<i>d</i>;3,4-<i>d</i>']bis[1,3]dioxol-4-yl ester

Synonyms:phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

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Technology Process of phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

There total 1 articles about phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 538-37-4
dibenzyl phosphochloridate

: 229612-81-1
1,2:3,4-di-O-isopropylidene-5S-(+)-proto-quercitol

: 913620-75-4
phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

Guidance literature:: With pyridine; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2006.06.096

Reference yield:

: 913620-75-4
phosphoric acid dibenzyl ester 2,2,7,7-tetramethyl-hexahydro-benzo[1,2-d;3,4-d']bis[1,3]dioxol-4-yl ester

: D-6-deoxy-myo-inositol-1-monophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol / 20 °C

2: cyclohexylamine; Dowex 50W*2 (H⁺) resin

With Dowex 50W*2 (H⁺) resin; hydrogen; cyclohexylamine; platinum(IV) oxide; In ethanol;
DOI:10.1016/j.bmcl.2006.06.096