C₂₂H₁₆⁽²⁾HNO₃S

Base Information

Chemical Name:C₂₂H₁₆⁽²⁾HNO₃S
CAS No.:1432521-64-6
Molecular Formula:C₂₂H₁₇NO₃S
Molecular Weight:376.44
Hs Code.:

C<sub>22</sub>H<sub>16</sub><sup>(2)</sup>HNO<sub>3</sub>S

Synonyms:C₂₂H₁₆⁽²⁾HNO₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₆⁽²⁾HNO₃S

Chemical Property:

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Technology Process of C₂₂H₁₆⁽²⁾HNO₃S

There total 3 articles about C₂₂H₁₆⁽²⁾HNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26340-47-6
3-Iodo-1H-indole

: 1432521-63-5
2-bromobenzaldehyde-α-d

: 1432521-64-6
C₂₂H₁₆⁽²⁾HNO₃S

Guidance literature:: With triphenylphosphine; cesium fluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 90 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.001

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1432521-64-6
C₂₂H₁₆⁽²⁾HNO₃S

Guidance literature:: Multi-step reaction with 3 steps

1: water-d2; potassium cyanide / diethyl ether / 68 h / 20 °C / Inert atmosphere

2: dichloro bis(acetonitrile) palladium(II); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; triethylamine / 1,4-dioxane / 110 °C / Inert atmosphere

3: bis(dibenzylideneacetone)-palladium⁽⁰⁾; triphenylphosphine; cesium fluoride / 1,2-dimethoxyethane / 16 h / 90 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium cyanide; dichloro bis(acetonitrile) palladium(II); water-d2; triethylamine; triphenylphosphine; cesium fluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; 1,2-dimethoxyethane; diethyl ether; 3: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2013.01.001

Reference yield:

: 59151-16-5
2-bromobenzaldehyde-α-d₁

: 1432521-64-6
C₂₂H₁₆⁽²⁾HNO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro bis(acetonitrile) palladium(II); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; triethylamine / 1,4-dioxane / 110 °C / Inert atmosphere

2: bis(dibenzylideneacetone)-palladium⁽⁰⁾; triphenylphosphine; cesium fluoride / 1,2-dimethoxyethane / 16 h / 90 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine; triphenylphosphine; cesium fluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; 1,2-dimethoxyethane; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2013.01.001