N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide

Base Information

• Chemical Name: N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide
• CAS No.: 609816-24-2
• Molecular Formula: C₂₁H₁₂F₁₇NO₂
• Molecular Weight: 633.305
• Mol file: 609816-24-2.mol

Synonyms:N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide

Chemical Property of N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide

There total 1 articles about N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

maleic anhydride (108-31-6) + 4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzylamine → N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide (609816-24-2)

Guidance literature:

maleic anhydride; 4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzylamine; In toluene; at 20 ℃; for 12h;

With zinc dibromide; In toluene; at 80 ℃; for 0.5h;

With 1,1,1,3,3,3-hexamethyl-disilazane; In toluene; at 80 ℃; for 4h;

DOI:10.1021/ol035214a

Reference yield: 96.0%

cyclohexa-1,3-diene (1165952-91-9) + N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide (609816-24-2) → (3aα,4α,7α,7aα)-2-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)-4,7-ethano-3a,4,7,7a-tetrahydro-1H-isoindole-1,3-dione

Guidance literature:

In 1,2-dichloro-ethane; at 60 ℃; for 48h;

DOI:10.1021/ol035214a

Reference yield: 93.0%

anthracene (120-12-7) + N-(4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)maleimide (609816-24-2) → 2,3:5,6-dibenzobicyclo[2.2.2]octane-7,8-(N-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzyl)dicarboxylic imide

Guidance literature:

In toluene; at 120 ℃; for 24h; under 1520 Torr;

DOI:10.1021/ol035214a

upstream raw materials:

maleic anhydride