C₄₉H₄₆BrN₃O₇

Base Information

Chemical Name:C₄₉H₄₆BrN₃O₇
CAS No.:1592908-17-2
Molecular Formula:C₄₉H₄₆BrN₃O₇
Molecular Weight:868.824
Hs Code.:

C<sub>49</sub>H<sub>46</sub>BrN<sub>3</sub>O<sub>7</sub>

Synonyms:C₄₉H₄₆BrN₃O₇

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Chemical Property of C₄₉H₄₆BrN₃O₇

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Technology Process of C₄₉H₄₆BrN₃O₇

There total 11 articles about C₄₉H₄₆BrN₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1592908-16-1
A₁₂

: 14002-51-8
4-biphenyl-carboxylic acid chloride

: 1592908-17-2
C₄₉H₄₆BrN₃O₇

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201301769

Reference yield:

: 958138-35-7
C₁₅H₂₁NO₆

: 1592908-17-2
C₄₉H₄₆BrN₃O₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

4.1: water; triphenylphosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

5.2: 2.08 h / 0 °C / Inert atmosphere

6.1: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 0 °C / Inert atmosphere; Darkness

7.1: acetic acid; sodium cyanoborohydride / ethanol / 4 h / 20 °C / Inert atmosphere

8.1: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / dichloromethane / 20 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With morpholine; pyridine; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/ejoc.201301769

Reference yield:

: 1016896-54-0
(2S,3S)-ethyl-3-(allyloxycarbonylamino)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzofuran-2-carboxylate

: 1592908-17-2
C₄₉H₄₆BrN₃O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

3.1: water; triphenylphosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

4.2: 2.08 h / 0 °C / Inert atmosphere

5.1: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 0 °C / Inert atmosphere; Darkness

6.1: acetic acid; sodium cyanoborohydride / ethanol / 4 h / 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate / dichloromethane / 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With morpholine; pyridine; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; tetrabutyl ammonium fluoride; water; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/ejoc.201301769