benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

Base Information

Chemical Name:benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate
CAS No.:1008530-33-3
Molecular Formula:C₂₂H₂₆N₂O₃
Molecular Weight:366.46
Hs Code.:

Synonyms:benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

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Chemical Property of benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

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Technology Process of benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

There total 2 articles about benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 5267-64-1
(R)-2-amino-3-phenylpropanol

: 1008530-33-3
benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

Guidance literature:: (S)-N-(benzyloxycarbonyl)valine; With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; at -5 ℃; for 0.75h;

(R)-2-amino-3-phenylpropanol; In dichloromethane; at -5 - 20 ℃; for 2h;

With triethylamine; p-toluenesulfonyl chloride; In dichloromethane; for 15h; Further stages.; Heating;
DOI:10.1002/anie.200704257

Reference yield:

: [(S)-1-((R)-1-Hydroxymethyl-2-phenyl-ethylcarbamoyl)-2-methyl-propyl]-carbamic acid benzyl ester

: 1008530-33-3
benzyl (S)-1-((R)-4-benzyl-4,5-dihydrooxazol-2-yl)-2-methylpropylcarbamate

Guidance literature:: With dmap; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tet.2008.11.046