acetoxy-beta-ionone

Base Information

• Chemical Name: acetoxy-beta-ionone
• CAS No.: 57593-24-5
• Molecular Formula: C₁₅H₂₂O₃
• Molecular Weight: 250.338

Synonyms:acetoxy-beta-ionone

Chemical Property of acetoxy-beta-ionone

Chemical Property:

Purity/Quality:

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Technology Process of acetoxy-beta-ionone

There total 3 articles about acetoxy-beta-ionone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

(E)-β-ionone (79-77-6,14901-07-6) + lead(IV) tetraacetate (546-67-8) → acetoxy-beta-ionone (57593-24-5)

Guidance literature:

In benzene; for 12h; Heating;

DOI:10.1016/0040-4020(84)85054-1

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) + tetraethylammonium tosylate (733-44-8) → acetoxy-beta-ionone (57593-24-5)

Guidance literature:

In acetic acid;

Reference yield:

→ acetoxy-beta-ionone (57593-24-5)

Guidance literature:

β-Ionon, Pb(OAc)4;

DOI:10.1021/ja00847a043

upstream raw materials:

(E)-β-ionone

lead(IV) tetraacetate

tetraethylammonium tosylate

Downstream raw materials:

10-hydroxy-β-ionone

(t-butyldimethylsiloxy)-β-ionone

(2E,4E,6E,8E)-7-(tert-Butyl-dimethyl-silanyloxymethyl)-3-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraenal

(2E,4E,6E,8E)-7-(tert-Butyl-dimethyl-silanyloxymethyl)-3-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraenoic acid ethyl ester

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