[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

Base Information

Chemical Name:[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]
CAS No.:221891-36-7
Molecular Formula:C₃₉H₄₀N₄O₆
Molecular Weight:660.77
Hs Code.:

Synonyms:[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

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Chemical Property of [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

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Technology Process of [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

There total 2 articles about [2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6813-38-3
2,2'-Bipyridine-4,4'-dicarboxylic acid

: 221891-36-7
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂, PhCH₂NEt₃Cl / 1,2-dichloro-ethane / Heating

2: Et₃N / tetrahydrofuran; methanol

3: 38 percent / DMAP, pyridine

With pyridine; dmap; thionyl chloride; N-benzyl-N,N,N-triethylammonium chloride; triethylamine; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1039/a808491b

Reference yield:

: 72460-28-7
2,2'-bipyridyl-4,4'-dicarboxylic acid chloride

: 221891-36-7
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran; methanol

2: 38 percent / DMAP, pyridine

With pyridine; dmap; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1039/a808491b

Reference yield: 90.0%

: bis(2,2'-bipyridine)dichlororuthenium(II) dihydrate

: 221891-36-7
[2,2']bipyridinyl-4,4'-dicarboxylic acid 4-({3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-propyl}-amide) 4'-[(3-hydroxy-propyl)-amide]

: HOC₃H₆NHCOC₁₀N₂H₆CONHC₃H₆OC(C₆H₅)(C₆H₄OCH₃)2Ru(C₁₀N₂H₈)2⁽²⁺⁾*2PF₆^(1-)*2H₂O

Guidance literature:: In ethanol; according to: K. A. Oppermann, S. L. Mecklenburg and T. J. Meyer, Inorg.Chem., 1994, 33, 5295 in 95% EtOH;
DOI:10.1039/a808491b