ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

Base Information

Chemical Name:ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate
CAS No.:1422388-83-7
Molecular Formula:C₁₃H₁₂ClFN₂O₂
Molecular Weight:282.702
Hs Code.:

Synonyms:ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

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Chemical Property of ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

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Technology Process of ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

There total 5 articles about ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: ethyl 3-((3-chloro-2-fluorophenyl)amino)-2-nitrobut-2-enoate

: 122-51-0
orthoformic acid triethyl ester

: 1422388-83-7
ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

Guidance literature:: With platinum on activated charcoal; hydrogen; at 75 ℃; for 4h; Inert atmosphere;

Reference yield: 2.0%

: 51605-32-4
ethyl 4⁽⁵⁾-methylimidazole-5⁽⁴⁾-carboxylate

: 352535-82-1
(3-chloro-2-fluorophenyl) boronic acid

: 1422388-83-7
ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

: 1422386-13-7
ethyl 1-(3-chloro-2-fluorophenyl)-4-methyl-1H-imidazole-5-carboxylate

Guidance literature:: With copper(I) oxide; In methanol; for 20h;

Reference yield:

: 2106-04-9
3-chloro-2-fluoroaniline

: 1422388-83-7
ethyl 1-(3-chloro-2-fluorophenyl)-5-methyl-1H-imidazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 7 h / 20 °C

2: platinum on activated charcoal; hydrogen / 4 h / 75 °C / Inert atmosphere

With platinum on activated charcoal; hydrogen; In ethanol;