Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Base Information

Chemical Name:Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester
CAS No.:163964-63-4
Molecular Formula:C₂₅H₃₄O₅Si
Molecular Weight:442.627
Hs Code.:

Synonyms:Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

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Technology Process of Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

There total 3 articles about Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136136-22-6
((4R,5S)-5-(hydroxymethyl)-2,2-dimethyl-1,3-dioxolan-4-yl)methyl acetate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 163964-63-4
Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 6h; Ambient temperature;

Reference yield:

: 55904-12-6
((4R,5S)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-methanol

: 163964-63-4
Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / SAM II_. lipase / 48 h / Ambient temperature

2: 100 percent / imidazole / dimethylformamide / 6 h / Ambient temperature

With 1H-imidazole; SAM II_. lipase; In N,N-dimethyl-formamide;

Reference yield:

: 163964-60-1
((4R,5S)-2,2-dimethyl-1,3-dioxolane-4,5-diyl)bis(methylene) bis-(2,2-dimethylpropanoate)

: 163964-63-4
Acetic acid (4R,5S)-5-(tert-butyl-diphenyl-silanyloxymethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / KOH / methanol; H₂O / 3 h / Ambient temperature

2: 80 percent / SAM II_. lipase / 48 h / Ambient temperature

3: 100 percent / imidazole / dimethylformamide / 6 h / Ambient temperature

With 1H-imidazole; potassium hydroxide; SAM II_. lipase; In methanol; water; N,N-dimethyl-formamide;