2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

Base Information

Chemical Name:2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin
CAS No.:80947-23-5
Molecular Formula:C₂₀H₂₁N₃OS
Molecular Weight:351.472
Hs Code.:

Synonyms:2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

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Chemical Property of 2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

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Technology Process of 2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

There total 3 articles about 2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 80947-22-4
N¹-Aethoxycarbonyl-N²-(2-methyl-4-phenyl-1,2,3,4-tetrahydroisochinol-8-yl)-S-aethylisothioharnstoff

: 80947-23-5
2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

Guidance literature:: In N,N-dimethyl-formamide; at 145 ℃; for 0.5h;

Reference yield:

: 80947-21-3
N¹-Aethoxycarbonyl-N²-(2-methyl-4-phenyl-1,2,3,4-tetrahydroisochinol-8-yl)thioharnstoff

: 80947-23-5
2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

Guidance literature:: Multi-step reaction with 2 steps

1: 7.1 g / potassium carbonate / acetone / 24 h

2: 80 percent / dimethylformamide / 0.5 h / 145 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetone;

Reference yield:

: 24526-64-5
nomifensine

: 80947-23-5
2-Aethylthio-4-hydroxy-9-methyl-7-phenyl-7,8,9,10-tetrahydropyrido<4,3-h>chinazolin

Guidance literature:: Multi-step reaction with 3 steps

1: 61.5 g / CH₂Cl₂ / 2 h / Ambient temperature

2: 7.1 g / potassium carbonate / acetone / 24 h

3: 80 percent / dimethylformamide / 0.5 h / 145 °C

With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetone;