(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

Base Information

Chemical Name:(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one
CAS No.:1189524-43-3
Molecular Formula:C₃₅H₄₈O₇Si
Molecular Weight:608.847
Hs Code.:

Synonyms:(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

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Chemical Property of (S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

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Technology Process of (S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

There total 2 articles about (S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1209497-66-4
C₃₅H₅₀O₇Si

: 1189524-43-3
(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

Guidance literature:: C₃₅H₅₀O₇Si; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.75h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1002/chem.200902226

Reference yield: 81.0%

: 1189524-71-7
tert-butyl((4S)-4-(3-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)oxiran-2-yl)pentyloxy)diphenylsilane

: 1189524-43-3
(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

Guidance literature:: With tributylphosphine; palladium diacetate; In tert-butyl alcohol; for 1.5h; Inert atmosphere; Reflux;
DOI:10.1002/anie.200900522

Reference yield:

: 1189524-43-3
(S)-6-(tert-butyldiphenylsilyloxy)-1-(4-methoxy-2,5-bis(methoxymethoxy)-3-methylphenyl)-3-methylhexan-2-one

: 1189524-60-4
(S)-2-(5-(tert-butyldiphenylsilyloxy)pentan-2-yl)-6-methoxy-7-methylbenzofuran-5-ol

Guidance literature:: With trifluorormethanesulfonic acid; In ethanol; toluene; at 80 ℃; for 0.0833333h; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.200900522