3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

Base Information

Chemical Name:3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol
CAS No.:156605-37-7
Molecular Formula:C₂₀H₃₆O₆Si
Molecular Weight:400.588
Hs Code.:

Synonyms:3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

Chemical Property:

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Technology Process of 3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

There total 1 articles about 3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)-1(E/Z)-propenyl>benzyl alcohol

: 156605-37-7
3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

Guidance literature:: With sodium periodate; hydrazine; In tetrahydrofuran; ethanol; at 75 ℃; for 2h;
DOI:10.1021/jo00094a061

Reference yield: 84.0%

: 156605-37-7
3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

: 156605-38-8
3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzaldehyde

Guidance literature:: With manganese(IV) oxide; In chloroform; at 50 ℃; for 1h;
DOI:10.1021/jo00094a061

Reference yield:

: 156605-37-7
3,4-Bis(methoxymethoxy)-5-<3-(tert-butyldimethylsiloxy)propyl>benzyl alcohol

: 3,4-Dihydroxy-5-(3-hydroxy-propyl)-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / MnO₂ / CHCl₃ / 1 h / 50 °C

2: 2 N AcOH / 20 h / 80 °C

With manganese(IV) oxide; acetic acid; In chloroform;
DOI:10.1021/jo00094a061