C₂₁H₂₄BrNO₃Si

Base Information

Chemical Name:C₂₁H₂₄BrNO₃Si
CAS No.:1423701-47-6
Molecular Formula:C₂₁H₂₄BrNO₃Si
Molecular Weight:446.416
Hs Code.:

C<sub>21</sub>H<sub>24</sub>BrNO<sub>3</sub>Si

Synonyms:C₂₁H₂₄BrNO₃Si

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Chemical Property of C₂₁H₂₄BrNO₃Si

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Technology Process of C₂₁H₂₄BrNO₃Si

There total 5 articles about C₂₁H₂₄BrNO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1423701-44-3
C₂₃H₂₈BrNO₃Si

: 1423701-47-6
C₂₁H₂₄BrNO₃Si

Guidance literature:: C₂₃H₂₈BrNO₃Si; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 80 ℃; for 20h;

With hydrogenchloride; In water;

Reference yield:

: 26510-95-2
ethyl 4-Bromobenzoylacetate

: 1423701-47-6
C₂₁H₂₄BrNO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: acetic acid; iron / ethanol / 100 °C

3: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

4: water; sodium hydroxide / methanol; tetrahydrofuran / 20 h / 80 °C

With water; iron; sodium hydride; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1423701-47-6
C₂₁H₂₄BrNO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 20 °C

2: acetic acid; iron / ethanol / 100 °C

3: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

4: water; sodium hydroxide / methanol; tetrahydrofuran / 20 h / 80 °C

With water; iron; sodium hydride; potassium carbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;