Technology Process of C16H24NO14P3
There total 3 articles about C16H24NO14P3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium hydroxide; water;
at 20 ℃;
for 20h;
DOI:10.1021/ja207907d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: iodine; silver nitrate / methanol / 20 °C
2.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / 2 h / -15 - -10 °C / Inert atmosphere
2.2: -10 - 0 °C / Inert atmosphere
2.3: 0 °C / pH 7.5
3.1: ammonium hydroxide; water / 20 h / 20 °C
With
trimethyl phosphite; ammonium hydroxide; water; iodine; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; silver nitrate; trichlorophosphate;
In
methanol;
DOI:10.1021/ja207907d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trimethyl phosphite; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate / 2 h / -15 - -10 °C / Inert atmosphere
1.2: -10 - 0 °C / Inert atmosphere
1.3: 0 °C / pH 7.5
2.1: ammonium hydroxide; water / 20 h / 20 °C
With
trimethyl phosphite; ammonium hydroxide; water; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trichlorophosphate;
DOI:10.1021/ja207907d