Technology Process of C17H19N5O3
There total 6 articles about C17H19N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap; triethylamine / tetrahydrofuran / Reflux
2: potassium phosphate; tetrakis(triphenylphosphine) palladium(0); XPhos / 1,4-dioxane; water / 19 h / 80 °C / Inert atmosphere
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h
4: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 21 h
5: trifluoroacetic acid / dichloromethane / 1 h
With
dmap; potassium phosphate; tetrakis(triphenylphosphine) palladium(0); lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; trifluoroacetic acid; XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
2: |Suzuki Coupling / 3: |Mitsunobu Displacement;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate; tetrakis(triphenylphosphine) palladium(0); XPhos / 1,4-dioxane; water / 19 h / 80 °C / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h
3: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 21 h
4: trifluoroacetic acid / dichloromethane / 1 h
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
1: |Suzuki Coupling / 2: |Mitsunobu Displacement;