2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

Base Information

Chemical Name:2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide
CAS No.:1259007-25-4
Molecular Formula:C₁₇H₁₄Cl₂N₄OS
Molecular Weight:393.296
Hs Code.:

Synonyms:2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

Chemical Property:

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Technology Process of 2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

There total 6 articles about 2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.7%

: 1338831-07-4
2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)acetic acid

: 95-53-4
o-toluidine

: 1259007-25-4
2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

Guidance literature:: 2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)acetic acid; With phosphorus pentachloride; In diethyl ether; at 20 ℃; for 2h; Cooling with ice;

o-toluidine; With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2011.08.011

Reference yield:

: 106103-85-9
2-(2-(2,4-dichlorophenyl)hydrazono)acetic acid

: 1259007-25-4
2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / toluene / 1 h / Reflux

2.1: trichlorophosphate / 10 h / Reflux

3.1: sodium hydride / tetrahydrofuran / 8.17 h / 0 °C / Reflux

4.1: sodium hydroxide / water; dimethyl sulfoxide / 1 h / 20 °C

5.1: phosphorus pentachloride / diethyl ether / 2 h / 20 °C / Cooling with ice

5.2: 2 h / 20 °C

With phosphorus pentachloride; sodium hydride; triethylamine; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide; toluene;
DOI:10.1016/j.ejmech.2011.08.011

Reference yield:

: 1259007-33-4
5-chloro-1-(2,4-dichlorophenyl)-1H-1,2,4-triazole

: 1259007-25-4
2-(2-(2,4-dichlorophenyl)-2H-1,2,4-triazol-3-ylthio)-N-o-tolylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 8.17 h / 0 °C / Reflux

2.1: sodium hydroxide / water; dimethyl sulfoxide / 1 h / 20 °C

3.1: phosphorus pentachloride / diethyl ether / 2 h / 20 °C / Cooling with ice

3.2: 2 h / 20 °C

With phosphorus pentachloride; sodium hydride; sodium hydroxide; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2011.08.011