(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Base Information

Chemical Name:(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole
CAS No.:503550-01-4
Molecular Formula:C₂₄H₃₁NO₄
Molecular Weight:397.514
Hs Code.:

Synonyms:(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Suppliers and Price of (2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

There total 4 articles about (2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 65-85-0,8013-63-6
benzoic acid

: 503550-00-3
(2S,3R,3aS,4aS,5R,8S,8aR)-3-(hydroxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

: 503550-01-4
(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F

Reference yield:

: 1560-11-8
cyclopent-1-enecarboxylic acid

: 503550-01-4
(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 98 percent / 4-(dimethylamino)pyridine; dicyclohexylcarbodiimide / CH₂Cl₂ / 24 h / 20 °C

2.1: calcium carbonate / toluene / 4 h / 45 °C

2.2: 50 percent / CH₂Cl₂ / 16 h / 60 °C

3.1: 93 percent / lithium aluminum hydride / diethyl ether / 1 h / 0 °C

4.1: 80 percent / dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h / 20 °C

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; calcium carbonate; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F

Reference yield:

: 87995-31-1
benzyl 1-cyclopentene-1-carboxylate

: 503550-01-4
(2S,3R,3aS,4aS,5R,8S,8aR)-3-(benzoyloxymethyl)-5,10,10-trimethyl-5,8-methano-2,3-propano-octahydroisoxazolo[3,2-b]benzoxazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: calcium carbonate / toluene / 4 h / 45 °C

1.2: 50 percent / CH₂Cl₂ / 16 h / 60 °C

2.1: 93 percent / lithium aluminum hydride / diethyl ether / 1 h / 0 °C

3.1: 80 percent / dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h / 20 °C

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; calcium carbonate; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/1099-0690(200211)2002:21<3566::AID-EJOC3566>3.0.CO;2-F