3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

Base Information

Chemical Name:3-methyl-1-phenyl-2,3-dihydrophosphindole oxide
CAS No.:34868-20-7
Molecular Formula:C₁₅H₁₅OP
Molecular Weight:242.257
Hs Code.:

Synonyms:3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

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Chemical Property of 3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

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Technology Process of 3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

There total 3 articles about 3-methyl-1-phenyl-2,3-dihydrophosphindole oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34868-19-4
benzyl-[2-(2-methoxy-1-methyl-ethyl)-phenyl]-phenyl-phosphane

: 34868-20-7
3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HBr / acetic acid

2: aq. NaOH / Heating

With sodium hydroxide; hydrogen bromide; In acetic acid;
DOI:10.1021/ja00752a035

Reference yield:

: 34868-17-2
1-benzyl-3-methyl-1-phenyl-2,3-dihydro-1H-phosphindolium; bromide

: 34868-20-7
3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

Guidance literature:: With sodium hydroxide; Heating;
DOI:10.1021/ja00752a035

Reference yield:

: 4141-48-4
allyldiphenylphosphine oxide

: 34868-20-7
3-methyl-1-phenyl-2,3-dihydrophosphindole oxide

Guidance literature:: With hydrogen fluoride; antimony pentafluoride; at -20 ℃; for 0.25h; Sealed tube; Schlenk technique;
DOI:10.1002/anie.201811032