allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

Base Information

Chemical Name:allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)
CAS No.:364378-92-7
Molecular Formula:C₃₄H₄₁N₃O₁₃
Molecular Weight:699.712
Hs Code.:

Synonyms:allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

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Technology Process of allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

There total 1 articles about allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108-05-4,9003-20-7
vinyl acetate

: 245109-90-4
allyl (2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1->4)-methyl-2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate

: 364378-92-7
allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

Guidance literature:: allyl (2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-(1->4)-methyl-2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate; With trifluoroacetic acid; In dichloromethane; water; at 0 ℃; for 2h;

vinyl acetate; With lipase P from Pseudomonas cepacia; In toluene; at 37 ℃; for 36h;
DOI:10.1002/1099-0690(200107)2001:14<2727::aid-ejoc2727>3.0.co;2-8

Reference yield: 63.0%

: 364378-92-7
allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

: 616876-63-2
O-(methyl 2-O-acetyl-4-O-(2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranosyl)-3-O-benzyl-α,β-L-idopyranosuronate) trichloroacetimidate

: 364378-96-1
C₇₀H₇₈N₆O₂₄

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 0.333333h;
DOI:10.1002/1099-0690(200107)2001:14<2727::aid-ejoc2727>3.0.co;2-8

Reference yield: 50.0%

: 364378-92-7
allyl 6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosiduronate)

: 6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosyluronyl) trichloroacetimidate

: C₇₂H₈₂N₆O₂₅

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 0.166667h;
DOI:10.1002/1099-0690(200107)2001:14<2727::aid-ejoc2727>3.0.co;2-8