N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

Base Information

Chemical Name:N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin
CAS No.:116626-63-2
Molecular Formula:C₁₇H₂₁NO₄
Molecular Weight:303.358
Hs Code.:

Synonyms:N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

Chemical Property:

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Technology Process of N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

There total 8 articles about N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 116626-61-0
N-<(2,5-Dibenzyloxy-4-methyl-phenyl)-methyl>-2-(2,5-dibenzyloxy-4-methyl-phenyl)-ethylamin

: 116626-63-2
N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 760 - 3040 Torr; Ambient temperature;

Reference yield:

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

: 116626-63-2
N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / NH₄OAc / 5 h / Heating

2: LiAlH₄ / diethyl ether / 48 h / Ambient temperature

3: 96 percent / TosOH / toluene / Heating

4: 80 percent / LiAlH₄ / diethyl ether / 48 h / Ambient temperature

5: 94 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 760 - 3040 Torr / Ambient temperature

With lithium aluminium tetrahydride; ammonium acetate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; toluene;

Reference yield:

: 40930-92-5
(2,5-Dibenzyloxy-4-methyl-phenyl)-methanol

: 116626-63-2
N-<(2,5-Dihydroxy-4-methyl-phenyl)-methyl>-2-(2,5-dihydroxy-4-methyl-phenyl)-ethylamin

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / SOCl₂ / diethyl ether / 3 h / Heating

2: 65 percent / DMSO / 3 h / 40 °C

3: LiAlH₄ / diethyl ether / 48 h / Ambient temperature

4: 96 percent / TosOH / toluene / Heating

5: 80 percent / LiAlH₄ / diethyl ether / 48 h / Ambient temperature

6: 94 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 760 - 3040 Torr / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; hydrogen; toluene-4-sulfonic acid; dimethyl sulfoxide; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; toluene;