5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

Base Information

Chemical Name:5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester
CAS No.:183056-11-3
Molecular Formula:C₁₇H₁₈O₅
Molecular Weight:302.327
Hs Code.:

Synonyms:5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

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Chemical Property of 5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

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Technology Process of 5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

There total 4 articles about 5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 183056-13-5
(E)-5-[2-(5-benzyloxy-2-methoxyphenyl)ethenyl]-2-hydroxybenzoic acid methylester

: 183056-11-3
5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 16h;

Reference yield:

: 41489-76-3
methyl-5-formyl-2-hydroxybenzoate

: 183056-11-3
5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, diisopropylamine / 1.) hexane , THF, -50 deg C, 1 h, 2.) hexane, THF, -70 deg C, 1 h

2: 69 percent / H₂ / 10percent Pd/C / ethyl acetate / 16 h

With n-butyllithium; hydrogen; diisopropylamine; palladium on activated charcoal; In ethyl acetate;

Reference yield:

: 105170-17-0
5-benzyloxy-2-methoxy-benzyl bromide

: 183056-11-3
5-[2-(5-hydroxy-2-methoxyphenyl)ethyl]-2-hydroxybenzoic acid methylester

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 2 h / 80 °C

2: 1.) n-BuLi, diisopropylamine / 1.) hexane , THF, -50 deg C, 1 h, 2.) hexane, THF, -70 deg C, 1 h

3: 69 percent / H₂ / 10percent Pd/C / ethyl acetate / 16 h

With n-butyllithium; hydrogen; diisopropylamine; palladium on activated charcoal; In ethyl acetate; toluene;