(Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle

Base Information

• Chemical Name: (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle
• CAS No.: 115817-97-5
• Molecular Formula: C₂₁H₂₂N₂O₉S
• Molecular Weight: 478.48

Synonyms:(Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle

Chemical Property of (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle

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Technology Process of (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle

There total 2 articles about (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(N,N-dimethylamino ethoxycarbonyl methylene) amino-3 methoxy-2 o-methoxycarbonylbenzamido-2 thioxo-3 propanoate de methyle (107938-61-4,115817-95-3) + acrolein (107-02-8,25068-14-8) → (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle (115817-97-5)

Guidance literature:

With Amberlyte 15; hydroquinone; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4020(01)85101-2

Reference yield:

methyl N-(o-methoxycarbonylbenzoyl)methoxy(thiocarbamoyl)glycinate (90475-40-4) → (Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle (115817-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent

2: 70 percent / amberlyte 15, hydroquinone / CH₂Cl₂ / Ambient temperature

With Amberlyte 15; hydroquinone; In dichloromethane;

DOI:10.1016/S0040-4020(01)85101-2

Reference yield:

(Ethoxycarbonyl-4 formyl-5 6H-thiazine-1,3 yl-2)-2 methoxy-2, o-methoxycarbonylbenzamido-2 ethanoate de methyle (115817-97-5) → 2-[Methoxy-methoxycarbonyl-(2-methoxycarbonyl-benzoylamino)-methyl]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester (115817-99-7,115818-01-4)

Guidance literature:

With Amberlyte 15; sodium cyanoborohydride; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0040-4020(01)85101-2

upstream raw materials:

(N,N-dimethylamino ethoxycarbonyl methylene) amino-3 methoxy-2 o-methoxycarbonylbenzamido-2 thioxo-3 propanoate de methyle

acrolein

methyl N-(o-methoxycarbonylbenzoyl)methoxy(thiocarbamoyl)glycinate

Downstream raw materials:

2-[Methoxy-methoxycarbonyl-(2-methoxycarbonyl-benzoylamino)-methyl]-5-methyl-3,6-dihydro-2H-[1,3]thiazine-4-carboxylic acid ethyl ester

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