Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc

Base Information

• Chemical Name: Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc
• CAS No.: 134304-90-8
• Molecular Formula: C₆₉H₉₄Cl₃N₁₃O₂₄
• Molecular Weight: 1595.94

Synonyms:Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc

Chemical Property of Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc

Chemical Property:

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Technology Process of Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc

There total 1 articles about Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-((S)-2-Acetylamino-3-hydroxy-propionylamino)-N-{(S)-1-[(S)-1-((S)-1-azidocarbonyl-2-methyl-propylcarbamoyl)-ethylcarbamoyl]-ethyl}-succinamic acid benzyl ester + C42H57Cl3N8O15 (83550-80-5) → Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc (134304-90-8)

Guidance literature:

With 1-methyl-pyrrolidin-2-one; In N,N-dimethyl-formamide; at -10 ℃; for 48h; Yield given;

DOI:10.1248/cpb.39.752

Reference yield: 72.0%

Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH-Troc (134304-90-8) → Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH2 (134304-91-9)

Guidance literature:

With acetic acid; zinc; In N,N-dimethyl-formamide; 1) 4 deg C, 2 h, 2) r.t., 8 h;

DOI:10.1248/cpb.39.752

upstream raw materials:

C₄₂H₅₇Cl₃N₈O₁₅

Downstream raw materials:

Ac-Ser-Asp(OBzl)-Ala-Ala-Val-Asp(OBzl)-Thr-Ser-Ser-Glu(OBzl)-Ile-NHNH₂

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