{3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II)

Base Information

• Chemical Name: {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II)
• CAS No.: 1352626-20-0
• Molecular Formula: C₅₉H₇₀MgN₁₆O₉
• Molecular Weight: 1171.61

Synonyms:{3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II)

Chemical Property of {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II)

Chemical Property:

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Technology Process of {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II)

There total 2 articles about {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

5,6-dibutoxypyrazine-2,3-dicarbonitrile (729613-46-1) + 5,6-bis(4-(hydroxymethyl)phenoxy)pyrazine-2,3-dicarbonitrile (1238353-41-7) + butan-1-ol (71-36-3) → (2,3,9,10,16,17,23,24-octabutoxy-1,4,8,11,15,18,22,25-octaazaphthalocyanininato)magnesium(II) (730965-05-6) + {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II) (1352626-20-0)

Guidance literature:

With iodine; magnesium; for 2h; Reflux;

DOI:10.1002/ejoc.201100689

Reference yield: 25.0%

5,6-bis(4-(hydroxymethyl)phenoxy)pyrazine-2,3-dicarbonitrile (1238353-41-7) + butan-1-ol (71-36-3) → (2,3,9,10,16,17,23,24-octabutoxy-1,4,8,11,15,18,22,25-octaazaphthalocyanininato)magnesium(II) (730965-05-6) + {3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II) (1352626-20-0)

Guidance literature:

butan-1-ol; With iodine; magnesium; for 3h; Reflux;

5,6-bis(4-(hydroxymethyl)phenoxy)pyrazine-2,3-dicarbonitrile; for 2h; Reflux;

DOI:10.1002/ejoc.201100689

Reference yield: 32.0%

{3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyaninato}magnesium(II) (1352626-20-0) → 3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyanine (1352626-21-1)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1002/ejoc.201100689

upstream raw materials:

5,6-dibutoxypyrazine-2,3-dicarbonitrile

5,6-bis(4-(hydroxymethyl)phenoxy)pyrazine-2,3-dicarbonitrile

butan-1-ol

Downstream raw materials:

3,9,10,16,17,23,24-heptabutoxy-2-[4-(hydroxymethyl)phenoxy]-1,4,8,11,15,18,22,25-octaazaphthalocyanine

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