p-ethyl<α-13C>benzyl alcohol

Base Information

• Chemical Name: p-ethyl<α-13C>benzyl alcohol
• CAS No.: 56248-22-7
• Molecular Formula: C₉H₁₂O
• Molecular Weight: 137.183

Synonyms:p-ethyl<α-13C>benzyl alcohol

Chemical Property of p-ethyl<α-13C>benzyl alcohol

Chemical Property:

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Technology Process of p-ethyl<α-13C>benzyl alcohol

There total 1 articles about p-ethyl<α-13C>benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

p-ethylbenzoic acid → p-ethyl<α-13C>benzyl alcohol (56248-22-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Heating;

DOI:10.1021/ja00236a038

Reference yield: 97.0%

p-ethyl<α-13C>benzyl alcohol (56248-22-7) → p-ethyl<α-13C>benzyl chloride

Guidance literature:

With hydrogenchloride; Ambient temperature;

DOI:10.1021/ja00236a038

Reference yield:

p-ethyl<α-13C>benzyl alcohol (56248-22-7) → p-ethyl(α-13C)toluene

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / conc. HCl / Ambient temperature

2: 80 percent / NaBH₄ / dimethylsulfoxide / 6 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; In dimethyl sulfoxide;

DOI:10.1021/ja00236a038

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