N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide

Base Information

• Chemical Name: N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide
• CAS No.: 1009734-70-6
• Molecular Formula: C₂₁H₃₀N₂O₄SSi
• Molecular Weight: 434.632

Synonyms:N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide

Chemical Property of N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide

Chemical Property:

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Technology Process of N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide

There total 1 articles about N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

tert-butyl [({(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yloxy}amino)sulfonyl]carbamate (1009734-69-3) → N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide (1009734-70-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 20h;

DOI:10.1021/jo701873t

Reference yield: 81.0%

C10H15NOS2 (1009734-76-2) + N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide (1009734-70-6) → N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]cyclohexane-carboxamide (1009734-75-1)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo701873t

Reference yield: 71.0%

N-{[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}sulfamide (1009734-70-6) + 3-isobutanoyl-thiazolidine-2-thione (151699-17-1) → N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]-2-methylpropanamide (1009734-73-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo701873t

upstream raw materials:

tert-butyl [({(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yloxy}amino)sulfonyl]carbamate

Downstream raw materials:

N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]cyclohexane-carboxamide

N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]acetamide

N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]-2-methylpropanamide

N-[({[(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl]oxy}amino)sulfonyl]hexanamide

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