(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

Base Information

Chemical Name:(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt
CAS No.:40719-44-6
Molecular Formula:C₁₂H₂₃N*C₂₉H₂₈N₂O₆
Molecular Weight:681.872
Hs Code.:

(<i>S</i>)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

Synonyms:(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

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Chemical Property of (S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

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Technology Process of (S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

There total 1 articles about (S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21240-34-6
4,5-diphenyl-1,3-dioxol-2-one

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 40719-44-6
(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

Guidance literature:: Multistep reaction; (i) OH, MeOH, (ii) /BRN= 1114120/, DMF, (iii) CF3CO2H, (iv) /BRN= 605923/, EtOH, Et2O;
DOI:10.1021/jo00957a024

Reference yield:

: 40719-44-6
(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

: 40719-47-9
(S)-2-amino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jo00957a024

Reference yield:

: 40719-44-6
(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoic acid; dicyclohexylamine salt

: 40719-56-0
N-[(S)-2-benzyloxycarbonylamino-6-(2-oxo-4,5-diphenyl-oxazol-3-yl)-hexanoyl]-glycine; dicyclohexylamine salt

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 1-ethyl-3-(3-dimethylamino-propyl)-carbodiimide*HCl / CH₂Cl₂

2: (i) aq. NaOH, dioxane, (ii) /BRN= 605923/, Et₂O, EtOH

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00957a024