(1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione

Base Information

• Chemical Name: (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione
• CAS No.: 98652-89-2
• Molecular Formula: C₂₈H₂₃NO₄
• Molecular Weight: 437.495

Synonyms:(1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione

Chemical Property of (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione

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Technology Process of (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione

There total 3 articles about (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14,15-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone (26307-17-5) + (1α,2α,3β,5β,6α,7α)-1,7-dibromo-9-methyl-4-oxa-9-azatetracyclo<5.3.0.02,6.03,5>decane-6,8-dione (98652-87-0) → (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.18,11.01,7.02,6.03,5>pentadec-9-ene-12,14,15-trione (98652-89-2)

Guidance literature:

With silver; zinc; In tetrahydrofuran; for 1h; Heating;

Reference yield: 71.0%

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone (26307-17-5) + C9H7NO3 (98652-88-1) → (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.18,11.01,7.02,6.03,5>pentadec-9-ene-12,14,15-trione (98652-89-2)

Guidance literature:

DOI:10.1021/ja00310a071

Reference yield:

(1α,2α,3β,5β,6α,7α)-1,7-dibromo-9-methyl-4-oxa-9-azatetracyclo<5.3.0.02,6.03,5>decane-6,8-dione (98652-87-0) → (1α,2β,3α,5α,6β,7α,8β,11β)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.18,11.01,7.02,6.03,5>pentadec-9-ene-12,14,15-trione (98652-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn/Ag

2: 71 percent

With silver; zinc;

DOI:10.1021/ja00310a071

upstream raw materials:

2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone

(1α,2α,3β,5β,6α,7α)-1,7-dibromo-9-methyl-4-oxa-9-azatetracyclo<5.3.0.0^2,6.0^3,5>decane-6,8-dione

C₉H₇NO₃

Downstream raw materials:

2,4,7-trimethyl-5,6-diphenyl-1H-isoindole-1,3(2H)-dione

(1α,2β,3α,5α,7α,8β,11β,15β)-15-hydroxy-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azahexacyclo<5.4.3.1^8,11.0^1,7.0^2,6.0^3,5>pentadec-9-ene-12,14-dione

(1α,2β,3α,5α,6β,7α)-8,11,13-trimethyl-9,10-diphenyl-4-oxa-13-azapentacyclo<5.4.3.0^1,7.0^2,6.0^3,5>tetradeca-8,10-diene-12,14-dione

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