N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

Base Information

Chemical Name:N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide
CAS No.:1037307-72-4
Molecular Formula:C₃₇H₅₇N₃O₁₂
Molecular Weight:735.872
Hs Code.:

N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

Synonyms:N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

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Chemical Property of N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

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Technology Process of N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

There total 1 articles about N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1037307-71-3
N-[(1S,2S)-2-tert-butyldiphenylsiloxy-1-tert-butoxycarbonyl-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

: 1037307-72-4
N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 168h;
DOI:10.1016/j.bmc.2008.03.020

Reference yield:

: 1037307-72-4
N-[(1S,2S)-1-tert-butoxycarbonyl-2-hydroxy-3-butenyl]-N-methyl-2-benzyloxycarbonylamino-3-O-[5-tert-butoxycarbonylamino-5-deoxy-2,3-O-(3-pentylidene)-β-D-ribofuranosyl]-2-hydroxybutanamide

: 57-10-3
1-hexadecylcarboxylic acid

: 1037307-73-5
C₅₃H₈₇N₃O₁₃

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2008.03.020