C₄₄H₇₀O₅Si₃

Base Information

Chemical Name:C₄₄H₇₀O₅Si₃
CAS No.:1261152-45-7
Molecular Formula:C₄₄H₇₀O₅Si₃
Molecular Weight:763.293
Hs Code.:

C<sub>44</sub>H<sub>70</sub>O<sub>5</sub>Si<sub>3</sub>

Synonyms:C₄₄H₇₀O₅Si₃

Suppliers and Price of C₄₄H₇₀O₅Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₄H₇₀O₅Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₄H₇₀O₅Si₃

There total 1 articles about C₄₄H₇₀O₅Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1261152-44-6
C₃₂H₄₂O₅Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1261152-45-7
C₄₄H₇₀O₅Si₃

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield: 80.0%

: 1261152-45-7
C₄₄H₇₀O₅Si₃

: 1261152-46-8
C₃₈H₅₆O₅Si₂

Guidance literature:: With 10-camphorsufonic acid; In methanol; at 25 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja109533y

Reference yield:

: 1261152-45-7
C₄₄H₇₀O₅Si₃

: 1261152-35-5
C₇₀H₉₈O₉Si₃

Guidance literature:: Multi-step reaction with 17 steps

1.1: 10-camphorsufonic acid / methanol / 3 h / 25 °C / Inert atmosphere

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 25 °C / Inert atmosphere; Molecular sieve

3.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

3.2: -78 - 0 °C / Inert atmosphere

4.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 3 h / 25 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 1 h / 25 °C / Inert atmosphere

6.1: bis(cyclohexanyl)borane / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

6.2: 1 h / 0 °C / Inert atmosphere

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 3 h / 25 °C / Inert atmosphere

8.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

9.1: dmap; 2-methyl-6-nitrobenzoic anhydride; triethylamine / toluene / 0.33 h / 25 °C / Inert atmosphere; Molecular sieve

9.2: 13 h / 25 °C / Inert atmosphere; Molecular sieve

10.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.67 h / 0 °C / Inert atmosphere

11.1: N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride / tetrahydrofuran; dichloromethane / 0 - 25 °C / Inert atmosphere

11.2: 0.67 h / 25 °C / Inert atmosphere

12.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

13.1: bis(cyclohexanyl)borane / tetrahydrofuran / 6 h / 25 °C / Inert atmosphere

13.2: 20 h / 0 °C / Inert atmosphere

14.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 25 °C / Inert atmosphere

15.1: p-toluenesulfonic acid monohydrate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

16.1: zinc trifluoromethanesulfonate / dichloromethane / 16 h / 25 °C / Inert atmosphere

17.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 30 °C / Inert atmosphere

17.2: -78 - 0 °C / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrapropylammonium perruthennate; 2-methyl-but-2-ene; N,N,N,N,-tetramethylethylenediamine; bis(cyclohexanyl)borane; 10-camphorsufonic acid; 2-methyl-6-nitrobenzoic anhydride; p-toluenesulfonic acid monohydrate; sodium hexamethyldisilazane; titanium tetrachloride; zinc trifluoromethanesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; toluene; tert-butyl alcohol; 3.1: Wittig reaction / 3.2: Wittig reaction / 6.1: Hydroboration reaction / 13.1: Hydroboration reaction;
DOI:10.1021/ja109533y